Organic Structure Determination Using 2-D NMR Spectroscopy
Academic Press Inc (Verlag)
978-0-12-088522-0 (ISBN)
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Organic Structure Determination Using 2-D NMR Spectroscopy is a primary text for a course in NMR techniques, with the goal to learn to identify organic molecular structure. It presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra.
It contains 20 known and 20 unknown structure determination problems and features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing. Many other books describe the methods used, but none offer a large number of problems. Instructors at universities and colleges are forced to cobble together problems from a wide range of sources. The fragmentary approach to assembling course materials has a negative impact on course continuity and thus adversely impacts student retention.
This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.
Jeffrey H Simpson, PhD, was Director of the Instrumentation Facility in the Department of Chemistry at M.I.T. from 2006 to 2017. Dr. Simpson’s career in NMR/instrumentation research and instruction spans 20 years, and he has authored an introductory text on the subject of NMR as well as publishing a number of peer-reviewed articles. He is one of the Founding Members of the New England NMR Society and served as VP from its inception to 2017. He currently is a faculty member in the Department of Chemistry at the University of Richmond.
PART I: Background and Methods
Chapter 1: Introduction
Chapter 2: Instrumental Considerations
Chapter 3: Data Collection, Processing, and Plotting
Chapter 4: 1H and 13C Chemical Shifts
Chapter 5: Symmetry and Topicity
Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling
Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE)
Chapter 8: Molecular Dynamics
Chapter 9: Strategies for Assigning Molecules
Chapter 10: Strategies for Elucidating Unknown Molecular Structures
PART II: Problems
Chapter 11 Simple Assignment Problems
Chapter 12: Complex Assignment Problems
Chapter 13: Simple Unknown Problems
Chapter 14: Complex Unknown Problems
| Erscheint lt. Verlag | 29.8.2008 |
|---|---|
| Verlagsort | San Diego |
| Sprache | englisch |
| Maße | 191 x 235 mm |
| Gewicht | 790 g |
| Themenwelt | Naturwissenschaften ► Biologie ► Genetik / Molekularbiologie |
| Naturwissenschaften ► Chemie ► Anorganische Chemie | |
| Naturwissenschaften ► Chemie ► Organische Chemie | |
| ISBN-10 | 0-12-088522-0 / 0120885220 |
| ISBN-13 | 978-0-12-088522-0 / 9780120885220 |
| Zustand | Neuware |
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