Process Engineering (eBook)

Addressing the Gap between Study and Chemical Industry

Michael Kleiber (Autor)

eBook Download: EPUB

2023 | 3rd, Revised and Extended Edition
574 Seiten
De Gruyter (Verlag)
978-3-11-102929-0 (ISBN)

Infos

'Reading the book, you can feel the long practical experience of the author. The text is easy to read, even where concepts can be complex. The strong theoretical background of the author is well known from other publications. In this book, however, the topics are presented on a level that every engineer and scientist in the chemical industry and process industry should know and can understand... This book would have been very helpful at the beginning of my career to close the addressed gap. Therefore, I can strongly recommend it not only to all students close to their degree, but also to engineers and scientists just starting their industrial career in the related industrial sectors that are subsumed under the term process industry (chemical or petrochemical industry, pharmaceutical industry, food industry, biochemical industry, environmental technology, etc.). The book is like an investment. Doing a better job and getting a better job evaluation might pay for the book ...' Prof. Dr.-Ing. Claus Fleischer, Frankfurt University of Applied Sciences

Process Engineering is based on almost 30 years of practical experience of the author in process simulation, design and development. The book is a missing link between students and practitioners. The author has coached many graduates in their first months and knows what the typical questions are.

Coming from the university, graduates often do not know which relevance their knowledge has and how to apply it in real life, whereas established practitioners often stick to the narrow way of their experience, forgetting that science continuously makes progress. There is a gap to be bridged.

From his own professional experience, the author covers many topics of the process engineering business, but three guest contributions are a valuable supplement to the content of the third edition. Already in the 2nd edition, Verena Haas from BASF SE wrote an excellent chapter on dynamic process simulation. For the new 3rd edition, Gökce Adali and Michael Benje added two chapters on digitalization and patents, respectively.

Preparing the reader for the everyday business!

Michael Kleiber started his career as a scientific assistant at the TU Brunswick, where he completed his doctoral thesis in 1994. He has worked for the former Hoechst AG and its successors in the fields of process development, process simulation and engineering calculations, before moving to ThyssenKrupp Uhde as a Chief Development Engineer. Dr. Kleiber is a member of the German Board of Thermodynamics and contributor to several standard works on process engineering, such as the VDI Heat Atlas, Winnacker-Kuechler and Ullmann's Encyclopedia of Industrial Chemistry.

Textauszug

1 Engineering projects

An engineering project is a huge and complex task for usually several hundred people. Coming from the university and just having finished one’s studies, one has usually no clue on what is going on beyond the own desk. In fact, the construction of a chemical plant is often compared to the erection of the pyramids in ancient Egypt. While the weight of a chemical plant is much lower, its complexity is by far greater, and the project can usually be completed in approx. three years instead of twenty. The target for a beginner must be to become a increasingly larger cog in the machine. First, an overview on the particular phases and activities must be obtained.

1.1 Process engineering activities

Plant engineering comprises the conceptual design, the scheduling and finally the erection of industrial plants. These industrial plants, in most cases built in chemical industry, are usually very complex, as manifold production steps are involved which are adjusted to each other. A number of specialists from different fields must be coordinated. A plant engineering project finishes with the commissioning and the proof of the guaranteed values.

A plant always belongs to somebody whose target is to quickly earn money by producing the substance the plant is designed for. At the beginning, a feasibility study has to be done. A market analysis is performed, which hopefully shows that it is worth starting a more detailed project. For a new process, it has to be checked whether it is possible to overcome the technical difficulties. The legal situation with patents and licenses has to be clarified, and possible locations for the plant are compared, whereby it is often necessary to consider different energy prices or transport costs for raw materials and products. A realistic production capacity and an impression of investment (CAPEX) and operation costs (OPEX) must be available before starting a project (Chapter 1.3). For the production capacity, it must be taken into account that no plant is in operation all the time; usually, 8000 h per year are scheduled, giving approx. 90 % availability. A corresponding overcapacity must be provided in the design.

It is important to know that an engineering project is not a sequential process, where e. g. first the reactors are planned and finished, then the product purification, and so on. This would actually be impossible, because due to recycle streams in the process a complete engineering design of a single part of the plant could never be achieved. Instead, all parts of the plant are worked out simultaneously, with increasing accuracy and degree of detailing. The advantage is that possible bottlenecks and difficulties are detected as early as possible, the interconnections are identified early, and an appropriate number of project participants can be assigned to work on the various parts of the plant. Certainly, this is not the way we are used to in everyday life, and there is often doubt as to whether it makes sense to perform a design of a piece of equipment while it is clear that the input streams are just preliminary and will change several times during the project. Nevertheless, as mentioned, it is most important to get an overview on the process as soon as possible. And with today’s tools, the design from the previous phase is usually an ideal starting point when the preconditions have been subject of change.

The engineering process is divided into certain phases, which are in principle:

• Conceptual Design

  Target: The process is fixed, the feasibility is checked, the risks are identified.

• Basic Engineering, also called FEED (Front End Engineering Design)

  Target: Preliminary elaboration of the plant, all documents available as good as possible

• Detailed Engineering

  Target: Complete and accurate description of all parts of the plant and all aspects of building.

Mixed forms (“Extended Basic”) and other denominations (“PDP”, i. e. Process Design Package) become more and more widespread. Finally, it depends on the contract which activities are comprised.

The process engineer should know what the follow-up activities of his calculations are. The first phase in a project is the conceptual design, where the first mass and energy balances are prepared, often based on lab trials and estimations.

The mass and energy balance is a key issue for all the following activities up to the phase of detailed engineering. A change in the mass balance has often a major impact on all other participants of the project, so it is desirable to make it as exact as possible, and to update it as soon as it makes sense. There is a certain misunderstanding as to what a mass and energy balance really is. The term “process simulation” is very common, and is also used here, but hardly applies. In fact, what the process does in the steady state for a given set of inlet conditions is calculated, i. e. the streams and the operating conditions of the particular pieces of equipment. Sometimes, the purpose is in fact to find out how the plant or the equipment behaves, at least how it reacts, and what the sensitivities are. However, in most cases, its purpose is to generate the data for the design of the equipment, applying conservative cases concerning process conditions or impurities. The exact process conditions that would enable the process engineer to really “simulate” the plant are usually not known, at least not in the Conceptual Design phase.

Despite these often occurring misunderstandings, “process simulation” is nowadays well acknowledged as a useful tool which requires a well-trained process engineer who has a profound knowledge of the process itself, its thermodynamics (Chapter 2), the various pieces of equipment and their peculiarities, and the simulation experience, in order to achieve convergence in the simulation flowsheet, which often turns out to be complex. Nowadays, some well-established commercial (ASPEN, HYSYS, ChemCAD, PRO/II, ProSim) and inhouse process simulators (Chemasim at BASF, VTPlan at Bayer) are available, performing calculations that would have been considered to be absolutely impossible 30 years ago. The genuine process simulation showing the actual plant behavior with respect to the design of the equipment, the startup-behavior, and the process control is called dynamic simulation (Chapter 3.7). Nowadays, its application becomes more and more popular, and conventional process simulation can be used as a starting point for the dynamic version.

Sometimes, single process steps remain unknown and are represented in the mass balance by simple split blocks. At least, there must be a concept of how to overcome this lack of knowledge and what the effort might be. At the beginning of the basic engineering these points should be completely clarified, and a full mass and energy balance must be available. How this is done is the subject of Chapters 2 and 3. It is desirable that pilot plant activities take place to confirm the mass balance and to make sure of the influence of the recycle streams. The main purpose of such an activity is to see whether all components are regarded and whether none of them accumulates in the process.

Figure 1.1 Example for the detailing in a PFD.

The particular pieces of equipment are preliminarily designed according to the current knowledge so that it becomes clear what the critical pieces of equipment are, either because of their size or because of possible delivery limitations. As well, it must be considered whether the plant can be operated at reduced or increased capacity, which might be necessary for a certain period of time. Useful tools are the process flow diagrams (PFD), where the whole process is visualized, including the main control loops (Figure 1.1). A PFD is a document to understand the process, operation data for the important streams and blocks are usually included. The counterpart of the PFD is process description, which describes the PFD in written form. It should not be excessively detailed, as its main purpose is to enable the reader to understand the essentials of the process. At the end of the conceptual design phase, equipment and operation costs and hence the feasibility and their basis are better defined, often with respect to a possible location.

In a so-called HAZID (HAZard IDentification) the main issues concerning the safety of the process are first discussed and listed, often with first recommendations. At a later stage, the so-called HAZOP will take place, where all relevant safety issues are discussed (Chapter 14.1). Finally, lists of utilities, raw products, auxiliary substances (e. g. catalysts) and emissions (exhaust air, waste water, solid and organic wastes) are issued. In the conceptual design phase, the design of the equipment can be done in a preliminary way using rules of thumb. A first optimization of the process should be performed. In process development, optimization is rarely a mathematical problem, where an objective function is defined and...

Produkt-Details

• Erscheint lt. Verlag: 20.11.2023
• Reihe/Serie: De Gruyter Textbook
• Reihe/Serie: De Gruyter Textbook
• Co-Autor: Gökce Adali, Michael Benje, Verena Haas
• Zusatzinfo: 60 b/w and 244 col. ill., 21 b/w tbl.
• Sprache: englisch
• Themenwelt: Technik ► Bauwesen
• Schlagworte: chemical engineering • Chemical Industry • chemical process engineering • Chemische Industrie • Industrial Chemistry • Technische Chemie • Verfahrenstechnik
• ISBN-10: 3-11-102929-8 / 3111029298
• ISBN-13: 978-3-11-102929-0 / 9783111029290