Multidimensional NMR Methods for the Solution State (eBook)

Gareth Morris, James W. Emsley (Herausgeber)

eBook Download: PDF

2012 | 1. Auflage
576 Seiten
John Wiley & Sons (Verlag)
978-1-118-58910-6 (ISBN)

Infos

The content of this volume has been added to
eMagRes (formerly Encyclopedia of Magnetic
Resonance) - the href="http://onlinelibrary.wiley.com/book/10.1002/9780470034590/homepage/rf_coils_virtual_issue.htm?cm=on-chem&cs=chem-analytic&cu=sitename-ln&cd=sitename-In-MRIgroup-VI"
target="_blank">ultimate online resource for NMR and MRI.

The literature of multidimensional NMR began with the
publication of three papers in 1975, then nine in 1976 and fifteen
in 1977, and now contains many tens of thousands of papers. Any
attempt to survey the field must therefore necessarily be very
selective, not to say partial. In assembling this handbook, the
Editors have sought to provide both the new researcher and the
established scientist with a solid foundation for the understanding
of multidimensional NMR, a representative if inevitably limited
survey of its applications, an authoritative account of classic
techniques such as COSY, NOESY and TOSCY, and an account of the
latest progress in the development of multidimensional
techniques.

This handbook is structured in four parts. The first opens with
an historical introduction to, and a brief account of, the
practicalities and applications of multidimensional NMR methods,
followed by a definitive survey of their conceptual basis and a
series of articles setting out the generic principles of methods
for acquiring and processing multidimensional NMR data. In the
second part, the main families of multidimensional techniques,
arranged in approximate order of increasing complexity, are
described in detail, from simple J-resolved spectroscopy through to
the powerful heteronuclear 3D and 4D methods that now dominate the
study of structural biology in solution. The third part offers and
illustrative selection from the very wide range of applications of
multidimensional NMR methods, including some of the most recent
developments in protein NMR. Finally, the fourth part introduces
the idea of multidimensional spectra containing non-frequency
dimensions, in which properties such as diffusion and relaxation
are correlated.

About EMR Handbooks / eMagRes
Handbooks

The Encyclopedia of Magnetic Resonance (up to 2012) and
eMagRes (from 2013 onward) publish a wide range of online
articles on all aspects of magnetic resonance in physics,
chemistry, biology and medicine. The existence of this large number
of articles, written by experts in various fields, is enabling the
publication of a series of EMR Handbooks / eMagRes
Handbooks on specific areas of NMR and MRI. The
chapters of each of these handbooks will comprise a carefully
chosen selection of articles from eMagRes. In consultation
with the eMagRes Editorial Board, the EMR
Handbooks / eMagRes Handbooks are coherently
planned in advance by specially-selected Editors, and new articles
are written (together with updates of some already existing
articles) to give appropriate complete coverage. The handbooks are
intended to be of value and interest to research students,
postdoctoral fellows and other researchers learning about the
scientific area in question and undertaking relevant experiments,
whether in academia or industry.

Have the content of this Handbook and the complete content of
eMagRes at your fingertips!

Visit: href="http://www.wileyonlinelibrary.com/ref/eMagRes">www.wileyonlinelibrary.com/ref/eMagRes

View other eMagRes publications href="http://onlinelibrary.wiley.com/book/10.1002/9780470034590/homepage/emagres_publications.htm"
target="_blank">here

Autor

Professor Gareth Morris, Department of Chemistry, The University of Manchester.

Inhalt

Contributors.

Series Preface.

Volume Preface.

Part A: Principles.

1 Multidimensional NMR: an Introduction (Gareth A. Morris,
James W. Emsley).

2 Multidimensional Spectroscopy: Concepts (Richard R.
Ernst).

3 Ultrafast Multidimensional NMR: Principles and Practice of
Single-Scan Methods (Maayan Gal, Lucio Frydman).

4 Fast Multidimensional NMR by Hadamard Spectroscopy (Ray
Freeman, Eriks Kupce).

5 Multidimensional NMR by Projection-Reconstruction (Ray
Freeman, Eriks Kupce).

6 Rapid Multidimensional NMR: Decomposition Methods and their
Applications (Martin Billeter, Doroteya K. Staykova).

7 Multidimensional Correlation Spectroscopy by Covariance NMR
(David A. Snyder, Rafael Bruschweiler).

8 Maximum Entropy Methods in Multidimensional NMR (Jeffrey C.
Hoch, Mehdi Mobli).

9 Filter Diagonalization Methods for Time-Domain Signals (A.
J. Shaka, Vladimir A. Mandelshtam).

10 Fourier Transform and Linear Prediction Methods (Jens J.
Led, Henrik Gesmar).

Part B: Techniques.

11 Two-Dimensional J-Resolved Spectroscopy (Gareth A.
Morris).

12 COSY (David M. Doddrell).

13 COSY: Quantitative Analysis (Alex D. Bain).

14 E.COSY: Determination of Coupling Constants (Harald
Schwalbe, P. Schmidt, Christian Griesinger).

15 Relayed Coherence Transfer Experiments (Philip H.
Bolton).

16 TOCSY (Timothy D. W. Claridge).

17 Multiple Quantum Spectroscopy of Liquid Samples (Timothy
J. Norwood).

18 NOESY (Michael P. Williamson).

19 ROESY (Ad Bax, Stephan Grzesiek).

20 TOCSY in ROESY and ROESY in TOCSY (J. Schleucher, J.
Quant, S. J. Glaser, Christian Griesinger).

21 2D Methods of Monitoring Exchange (Keith G.
Orrell).

22 Heteronuclear Shift Correlation Spectroscopy (Thomas T.
Nakashima, R. E. D. McClung).

23 2D Methods for the Measurement of Long-Range
Proton-Carbon Coupling Constants (Teodor Parella).

24 Homonuclear 3D NMR of Biomolecules Rolf Boelens, Robert
Kaptein).

25 3D HMQC-NOESY, NOESY-HMQC, and NOESY-HSQC (Ranjith
Muhandiram, Lewis E. Kay).

26 3D and 4D Heteronuclear Magnetic Resonance (G. Marius
Clore, Angela M. Gronenborn).

Part C: Applications.

27 2D Carbon-Heteroelement Correlation (Stefan
Berger).

28 Multidimensional NMR in Organotin Chemistry and Catalysis
(Monique Biesemans, Rudolph Willem).

29 2D NMR of Molecules Oriented in Liquid Crystalline Phases
(Anil Kumar).

30 2D NMR of Molecules Oriented in Liquid Crystals--Recent
Developments (Anil Kumar, N. Suryaprakash).

31 Local Field Experiments in Liquid Crystals (Stefano
Caldarelli).

32 Multiple Quantum Spectroscopy in Liquid Crystalline Solvents
(Leslie D. Field).

33 Biological Macromolecules: Structure Determination in
Solution (Kurt W¨uthrich).

34 Structures of Larger Proteins, Protein-Ligand, and
Protein-DNA Complexes by Multidimensional Heteronuclear NMR
(G. Marius Clore, Angela M. Gronenborn).

35 Rapid Multidimensional NMR: Fast Pulsing Techniques and their
Applications to Proteins (Bernhard Brutscher, Paul
Schanda).

Part D: Related Techniques.

36 Diffusion-Ordered Spectroscopy (Gareth A. Morris).

37 2D Relaxometry (Brian P. Hills).

Index.

Rezensionen

"This book is also very nicely produced, with a very good number of
beautifully coloured figures. There is a useful subject index and a
well organised and informative list of contributors, giving not
only both their research laboratory addresses but also again
stating, as well as the usual contents listing summary, their
chapter and topic contributions." (Crystallography Reviews, 9
August 2011)

Produkt-Details

• Erscheint lt. Verlag: 19.12.2012
• Reihe/Serie: EMR Books
• Reihe/Serie: EMR Books
• Sprache: englisch
• Themenwelt: Naturwissenschaften ► Chemie ► Analytische Chemie
• Themenwelt: Naturwissenschaften ► Physik / Astronomie
• Themenwelt: Technik
• Schlagworte: Chemie • Chemistry • NMR Spectroscopy / MRI / Imaging • NMR-Spektroskopie • NMR-Spektroskopie / MRT / Bildgebende Verfahren
• ISBN-10: 1-118-58910-6 / 1118589106
• ISBN-13: 978-1-118-58910-6 / 9781118589106