High Throughput Screening in Chemical Catalysis (eBook)

Technologies, Strategies and Applications

Alfred Hagemeyer, Peter Strasser, Jr. Volpe Anthony F. (Herausgeber)

eBook Download: PDF

2006 | 1. Auflage
XX, 319 Seiten
Wiley-VCH (Verlag)
978-3-527-60430-2 (ISBN)

Infos

In this first book to present every important aspect of this fascinating and developing field, the three editors A. Hagemeyer, P. Strasser and A. F. Volpe Jr. from Symyx Technologies have chosen a perfect mixture of distinguished, international authors from both academia and industry. Each chapter is devoted to a major topic - high-throughput experimentation methodologies, integrated combinatorial synthesis and screening workflow, and applications to chemical catalysts with an emphasis on heterogeneous catalysis, olefin polymerization and electrocatalysis for fuel cells. An indispensable source for everyone working in the field. Kombinatorische Strukturbibliotheken, verbunden mit Hochdurchsatz-Screeningverfahren, beschleunigen die Suche nach Verbindungen mit neuen, gewünschten Eigenschaften wesentlich. In diesem Band demonstriert ein internationales Autorenteam, wie man entsprechende Ansätze effektiv in die Praxis umsetzt. Am Beispiel der heterogenen Katalyse, der Polymerisation von Olefinen und der Elektrokatalyse für Brennstoffzellen werden Hochdurchsatz-Experimente, kombinatorische Synthese und Screening von vielen Seiten beleuchtet und diskutiert.

Autor

Alfred Hagemeyer received his diploma degrees in chemistry, 1985, and physics, 1987, from the university of Dortmund, Germany, did his Ph.D. at the Max-Planck-Institute fuer Polymerforschung in Mainz, Germany, 1987-1989, was postdoc at the university of Bologna, Italy, 1990, was employed at BASF, corporate research, ammonia laboratory, Ludwigshafen, Germany, 1991-1996, and at Hoechst/Aventis, corporate research, department of heterogeneous catalysis, Frankfurt, Germany, 1996-1998, and joined Symyx Technologies, heterogeneous catalysis group, Santa Clara, CA, in 1998 where he is a Distinguished Scientist. His research interests are in the area of gas and liquid-phase heterogeneous catalysis. He has about 30 publications and about 80 patents/patent applications. Anthony Volpe joined Symyx Technologies in 1999 and is currently the Director of the Heterogeneous Catalysis Group. Prior to joining Symyx, he was employed at Rohm and Haas in Spring House, PA for eight years in the Heterogeneous Catalysis group and in the Exploratory Polymers group. Dr. Volpe received his Ph.D. in organic chemistry in 1991 from the University of North Carolina at Chapel Hill under the direction of Professor Maurice Brookhart and his BA in chemistry in 1986 form Occidental College in Los Angeles. His research areas have included gas and liquid phase heterogeneous catalysis and homogeneous catalysis. He has approximately 30 publications and patents/patent applications. Peter Strasser studied chemistry at the University of Tuebingen, Germany, Stanford University, and University of Pisa, Italy. He received his diploma degree in 1995. He did his doctoral research work at the 'Fritz-Haber-Institut der Max-Planck-Gesellschaft' under the direction of Professor Gerhard Ertl, and received his Ph.D. in Physical Chemistry in 1999. He was visiting scientists with Sony Central Research in 1996. Dr. Strasser joined Symyx Technologies in 2000 and is currently Senior Staff Scientist in the Electronic Materials Group. His research interests are in the area of fuel cells, electrocatalysis and heterogeneous catalysis. He has about 25 publications and about 10 patents/patent applications.

Inhalt

INTRODUCTION
Impact of Combinatorial Methods and High Throughput Screening on Chemical Catalysis
TECHNOLOGY
Mastering the Challenges of Catalyst Screening in High Throughput Experimentation for Heterogeneously Catalyzed Gas Phase Reactions
High Throughput Workflow Development: Strategies and Examples in Heterogeneous Catalysis
Integrated Micro Reactor Set-ups for High-Throughput Screening and Methods for Analytical Evaluations of Low Density Screening Data
EXPERIMENT DESIGN/SCREENING STRATEGIES:
Two Exemplied Combinatorial Approaches for Catalytic Liquid/Solid and Gas/Solid Processes in Oil Refining and Fine Chemicals
Present Trends in the Application of Genetic Algorithms and Neural Networks to Heterogeneous Catalysis
DETECTION
Relative Quantification of Catalytic Activity in Combinatorial Libraries by Emissivity Corrected Infrared Thermography
Gas Sensor Technology for the High Throughput Screening in Catalysis
APPLICATIONS
Parallel approaches to the synthesis and testing of catalysts for liquid phase reactions
Combinatorial Strategies for Speeding up Discovery and Optimization of Heterogeneous Catalysts at Academic Lab Scale - Case Study of Hydrogeneous Purification for Feeding PEM Fuel Cells
Combinatorial and High Throughput Screening of Fuel Cell Electrocatalysts
High-Throughput Approaches in Olefin Polymerization Catalysis

INTRODUCTION
Impact of Combinatorial Methods and High Throughput Screening on Chemical Catalysis
TECHNOLOGY
Mastering the Challenges of Catalyst Screening in High Throughput Experimentation for Heterogeneously Catalyzed Gas Phase Reactions
High Throughput Workflow Development: Strategies and Examples in Heterogeneous Catalysis
Integrated Micro Reactor Set-ups for High-Throughput Screening and Methods for Analytical Evaluations of Low Density Screening Data
EXPERIMENT DESIGN/SCREENING STRATEGIES:
Two Exemplied Combinatorial Approaches for Catalytic Liquid/Solid and Gas/Solid Processes in Oil Refining and Fine Chemicals
Present Trends in the Application of Genetic Algorithms and Neural Networks to Heterogeneous Catalysis
DETECTION
Relative Quantification of Catalytic Activity in Combinatorial Libraries by Emissivity Corrected Infrared Thermography
Gas Sensor Technology for the High Throughput Screening in Catalysis
APPLICATIONS
Parallel approaches to the synthesis and testing of catalysts for liquid phase reactions
Combinatorial Strategies for Speeding up Discovery and Optimization of Heterogeneous Catalysts at Academic Lab Scale - Case Study of Hydrogeneous Purification for Feeding PEM Fuel Cells
Combinatorial and High Throughput Screening of Fuel Cell Electrocatalysts
High-Throughput Approaches in Olefin Polymerization Catalysis

Rezensionen

"... this book is definitely very stimulating and informative for everyone interested in the topics that are covered by the individual chapters."
Angewandte Chemie I.E.

"For anyone who wants to get a timely overview about the most fascinating approaches addressing the most relevant issues in modern catalysis, written by the leading experts in the field! These readers will not be disappointed and will enjoy reading this well-written book!"
Synthesis

"... für den am Thema interessierten Leser ... sehr informativ, lehrreich und vielleicht auch stimulierend ..."
Angewandte Chemie

Produkt-Details

• Erscheint lt. Verlag: 6.3.2006
• Sprache: englisch
• Themenwelt: Naturwissenschaften ► Chemie ► Organische Chemie
• Themenwelt: Technik
• Schlagworte: catalysis • Chemie • Chemische Technik • Chemistry • Katalyse • Lab Automation & Miniaturization • Laborautomatisierung u. Miniaturisierung • Methods - Synthesis & Techniques • Organische Chemie / Methoden, Synthesen, Verfahren • Physical Chemistry • Physikalische Chemie • spectroscopy • Spektroskopie
• ISBN-10: 3-527-60430-8 / 3527604308
• ISBN-13: 978-3-527-60430-2 / 9783527604302