Annual Reports on NMR Spectroscopy (eBook)

Graham A. Webb (Herausgeber)

eBook Download: PDF

2007 | 1. Auflage
312 Seiten
Elsevier Science (Verlag)
978-0-08-047587-5 (ISBN)

Infos

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy.

* Provides updates on the latest developments in NMR spectroscopy
* Includes comprehensive review articles
* Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy. - Provides updates on the latest developments in NMR spectroscopy- Includes comprehensive review articles- Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Inhalt

Cover 1
Copyright page 5
List of Contributors 6
Preface 8
Contents 10
Chapter 1. Resolution Enhancement in In Vivo NMR Spectroscopy 12
1. Introduction 13
2. Resolution in In Vivo MRS 16
3. Spatial Resolution 17
4. Temporal Resolution 19
5. Spectral Resolution 21
6. Conclusion 52
Acknowledgements 52
References 53
Chapter 2. Spin Echo NMR Diffusion Studies 62
1. Introduction 63
2. Fundamentals of Pulsed Field Gradient NMR Diffusion Studies 65
3. Review of PFG NMR Pulse Sequences 85
4. Generation and Application of High-Intensity Pulsed Field Gradients 102
5. Recent PFG NMR Diffusion Studies on Porous Materials 116
Acknowledgements 133
References 133
Chapter 3. Recent Advances in Theoretical Calculations of Indirect Spin–Spin Coupling Constants 144
1. Introduction 145
2. General Features of Spin–Spin Coupling Constants 146
3. Calculation of Spin–Spin Coupling Constants 170
4. Computational Results – An Illustrative Compilation and a Practical Guide. 203
Acknowledgements 245
References 245
Chapter 4. Solid-State NMR Studies on Semicrystalline Polymers 258
1. Introduction 258
2. Polyethylene and Ethylene Copolymers 259
3. Some other Semicrystalline Polymers 275
References 292
Chapter 5. Selective NMR Excitations in Chiral Analysis 294
1. Introduction 294
2. Selective Homonuclear Refocusing Experiments: SERF and SERFph 295
3. Combination of Variable Angle Sample Spinning and SERF or SERFph Experiments 299
4. Heteronuclear Selective Refocusing, HetSERF, Experiments 300
5. Conclusion 303
References 303
Index 306

Produkt-Details

• Erscheint lt. Verlag: 9.5.2007
• Sprache: englisch
• Themenwelt: Sachbuch/Ratgeber
• Themenwelt: Naturwissenschaften ► Chemie ► Analytische Chemie
• Themenwelt: Naturwissenschaften ► Chemie ► Organische Chemie
• Themenwelt: Naturwissenschaften ► Chemie ► Technische Chemie
• Themenwelt: Naturwissenschaften ► Physik / Astronomie ► Elektrodynamik
• Themenwelt: Technik ► Umwelttechnik / Biotechnologie
• ISBN-10: 0-08-047587-6 / 0080475876
• ISBN-13: 978-0-08-047587-5 / 9780080475875