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Inorganic Syntheses

Buch | Hardcover

223 Seiten

2006
John Wiley & Sons Inc (Verlag)
978-0-470-13178-7 (ISBN)

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The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Fred Basolo was an American inorganic chemist. He received his Ph.D. at the University of Illinois at Urbana-Champaign in 1943, under Prof. John C. Bailar, Jr. Basolo spent his professional career at Northwestern University.

Preface.
Notice to Contributors.

Chapter One Metal Nitrosyl Complexes.

1 Tetranitrosylchromium and Carbonyltrinitrosylmanganese.

2 Dithiocarbamate Complexes of Iron and Cobalt Nitrosyls.

3 Ammine Complexes of Osmium, Including Amminenitrosyls.

4 Nitrosylammineruthenium Complexes.

5 Dinitrosylcobalt Complexes.

6 Bis(triphenylphosphine)chlorodinitrosylruthenium(1+)
Tetrafluoroborate.

7 Dicarbonyl-?-cyclopentadienylnitrosylmolybdenum
and Bis(dihalo-?- cyclopentadienylnitrosylmolybdenum)
Derivatives.

8 Bis(methyldiphenylphosphine)dichloronitrosylcobalt.

9 Tris(triphenylphosphine)nitrosylcobalt and
Tris(triphenylphosphine)nitrosylrhodium.

10 Carbonylchloronitrosylrhenium Compounds.

11 Decacarbonyldi-?-nitrosyl-trimetal Compounds.

12 trans-Bis(triphenylphosphine)chloronitrosyliridium(1+)
Tetrafluoroborate.

Chapter Two Metal Carbonyl Compounds.

13 Dodecacarbonyltriruthenium.

14 Dodecacarbonyltriruthenium.

15 Hexadecacarbonylhexarhodium.

16
Di-?-chloro-bis[tricarbonylchlororuthenium(II)].

17
Dicarbonyl(?-cyclopentadienyl)(thiocarbonyl)manganese(I).

18 Transition Metal Carbonyl Derivatives of Magnesium.

19 Tris(pentacarbonylmanganese)thalium(III).

20 (Alkylamino)difluorophosphine- and
Halodifluorophosphinetetracarbonyliron Complexes.

21 Tris[bis(2-methoxyethyl)ether]potassium and
Tetraphenylarsonium Hexacarbonylmetallates(1?) of Niobium and
Tantalum.

Chapter Three Werner Type Metal Complexes.

22 (Dinitrogen oxide)pentaammineruthenium(II) Salts.

23 Tetrakis(isothiocyanato)bis(2.2'-bipyridine)niobium(IV).

24 Malonato Complexes of Chromium(III).

25 Selenoureametal Complexes.

26 Nickel Tetrafluorooxovanadate(IV) Heptahydrate.

27 Polymeric Chromium(III)-bis(phosphinates).

28 Resolution of the
cis-Bromoamminebis(ethylenediamine)cobalt(III) Ion.

29 Bis(alkylphosphine)trichlorotitanium(III) Complexes.

Chapter Four Other Transition Metal Complexes.

30 Reagents for the Synthesis of ?-Diene Complexes
of Tricarbonyliron and Tricarbonylruthenium.

31 Bis(?)-cyclopentadienylniobium Complexes.

32 Dichloro(1,3-propanediyl)platinum and
trans-Dicholorobis(pyridine)(1,3-propane-diyl)platinum
Derivatives.

33 Olefin(?)silver(I) Compounds.

34 Trichloromethyltitanium and Tribromomethyltitanium.

35 Ethylenebis(triphenylphosphine)palladium(0) and Related
Complexes.

Chapter Five Main-Group and Actinide Compounds.

36 Tetraethylammonium, Tetraphenylarsonium, and Ammonium
Cyanates and Cyanides.

37 Diindenylmagnesium.

38 Fluoromethylsilanes.

39 Uranium Hexachloride.

40 Cholorotris(?-cyclopentadienyl) Complexes of
Uranium(IV) and Thorium(IV).

Chapter Six Ligands Used to Prepare Metal Complexes.

41 Trimethylphosphine.

42 Tertiary Phosphines.

43 Diphenylphosphine.

44 Tri(phenyl-d3)phosphine.

45 Methyl Difluorophosphite.

46 Bi-, Tri-, and Tetradentate Phosphorus-Sulfur Ligands.

47 Tetradentate Tripod Ligands Containing Nitrogen, Sulfur,
Phosphorus, and Arsenic as Donor Atoms.

48 Dimethyl(pentafluorophenyl)phosphine and
Dimethyl(pentafluorophenyl)arsine Ligands.

49 Tris(?-dimethylarsinophenyl)arsine and
Tris(?-dimethylarsinophenyl)stibine.

50 cis-2-Diphenylarsinovinyldiphenylphosphine and
2-Diphenylarsinoethyldiphenylphosphine.

51 [2-(Isopropylphenylphosphino)ethyl]diphenylphosphine.

52 [(Phenylisopropylphosphino)methyl]diphenylphosphine
Sulfide.

53
N,N,N',N'-Tetrakis(diphenylphosphinomethyl)ethylenediamine.

54 Ethylenebis(nitrilodimethylene)tetrakis(phenylphosphinic
acid).

55 [2-(Phenylphosphino)ethyl]diphenylphosphine.

56 1,1,1-Trifluoro-4-mercapto-4-(2-thienyl)-3-buten-2-one.

Chapter Seven Compounds of Biological Interest.

57 Metalloporphyrins.

58 (1,4,8,11-Tetraazacyclotetradecane)nickel(II) Perchlorate and
1,4,8,11-Tetraazacyclotetradecane.

59 N,N'-Ethylenebis(monothiacetylacetoniminato)cobalt(II)
and Related Metal Complexes.

60 Metallatranes.

61
cis-Bis(diethyldithiocarbamato)dinitrosylmolybdenum.

62 Some ?-Cyclopentadienyl Complexes of
Titanium(III).

Index of Contributors.

Subject Index.

Formula Index.

Erscheint lt. Verlag	19.1.2011
Reihe/Serie	Inorganic Syntheses
Mitarbeit	Chef-Herausgeber: Fred Basolo
Verlagsort	New York
Sprache	englisch
Themenwelt	Naturwissenschaften ► Chemie ► Anorganische Chemie
ISBN-10	0-470-13178-0 / 0470131780
ISBN-13	978-0-470-13178-7 / 9780470131787
Zustand	Neuware