Continuous Preferential Crystallization of Enantiomers: Simulation, Analysis, Process Design and Experimental Validation

Kamila Galan (Autor)

Buch

140 Seiten

2017 | 1. Aufl.
docupoint (Verlag)
978-3-86912-219-9 (ISBN)

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Within this project, simulation studies are conducted to quantify the dynamics of the investigated process, its possible modifications as well as to find conditions under which steady states can be reached fast. Two different process configurations are investigated: a single MSMPR crystallizer and two MSMPR crystallizers coupled via an exchange of their mother liquors. The latter concept is applied and tested for the first time in a continuous operation. Based on the results of simulations, a favorable operating window is found, which is then experimentally validated.
Additionally, a suitable experimental pilot plant is constructed, where challenges connected with the product suspension removal are addressed. Finally, systematic experimental investigations are carried out to find process conditions, where a continuous resolution can be achieved under steady state operations.

Erscheinungsdatum	17.02.2017
Verlagsort	DE
Sprache	englisch
Einbandart	Paperback
Themenwelt	Naturwissenschaften ► Chemie ► Physikalische Chemie
ISBN-10	3-86912-219-6 / 3869122196
ISBN-13	978-3-86912-219-9 / 9783869122199
Zustand	Neuware