The Practice of NMR Spectroscopy

with Spectra-Structure Correlations for Hydrogen-1

Nugent Chamberlain (Autor)

Buch | Softcover

424 Seiten

2013 | Softcover reprint of the original 1st ed. 1974
Springer-Verlag New York Inc.
978-1-4757-1477-7 (ISBN)

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I. GENERAL When a sample containing hydrogen is placed in the Although it is assumed that the reader has been exposed static magnetic field, each hydrogen nucleus will precess to the elementary theory of NMR and to the operation at a frequency determined by the magnetic field it of an NMR spectrometer, a brief review of some of the actually experiences. This field, in turn, is determined by basic concepts and definitions will indicate the point of the electronic, and therefore the chemical, environment view used in this book and clarify some of the defini of the nucleus. Thus the variety of chemical environ tions. The discussion is confined to the hydrogen-l iso ments that exist in a molecule will produce a spectrum tope because this is by far the most generally used and, of precession frequencies that will indicate the chemical consequently, far more data are available for it than for nature of the various parts of the molecule. The remain any other isotope. This wealth of data, in turn, leads to ing problem is to observe this spectrum of frequencies. the most accurate and comprehensive set of spectra There are two general methods of observing the structure correlations. spectrum.

1 Introduction.- 2 Producing NMR Data.- 3 Analytical Procedures.- 4 Chemical Shift Correlations.- 5 Coupling Constant Correlations.- 6 Typical NMR Spectra.- Chemical Shift Correlation Charts.- The Index Chart I1.- The Summary Charts S1 to S35.- The Detailed Charts 1 to 89.- Coupling Constant Correlation Charts.- The Index Chart I2.- The Summary Charts J1 to J38.- Typical Spectra Plates 1 to 59.- References.- I. Introduction.- A. Organization.- B. Selection and Processing of Data.- II. Text References.- III. Acknowledgments.- IV. Data References—Major Sources.- A. Textbooks.- B. Catalogs of NMR Spectra.- C. Tabulations of NMR Data.- D. Chemical Shift Charts.- E. Theoretical Spectra.- F. Spectral Pattern Guide.- V. Data References—Scientific Papers.- A. Hydrocarbons.- B. Oxygen Compounds.- C. Halogen Compounds.- D. Nitrogen Compounds.- E. Sulfur Compounds.- F. Phosphorus Compounds.- G. Coupling Constants.- H. Strong Intramolecular Hydrogen Bonds.- Appendix—Filing System for NMR Spectra.- Author Index.

Zusatzinfo	1 Illustrations, black and white; XXIV, 424 p. 1 illus.
Verlagsort	New York, NY
Sprache	englisch
Maße	210 x 279 mm
Themenwelt	Naturwissenschaften ► Chemie ► Physikalische Chemie
ISBN-10	1-4757-1477-7 / 1475714777
ISBN-13	978-1-4757-1477-7 / 9781475714777
Zustand	Neuware