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Chemical Derivatization in Analytical Chemistry -

Chemical Derivatization in Analytical Chemistry

Chromatography

R. W. Frei (Herausgeber)

Buch | Softcover
344 Seiten
2012 | Softcover reprint of the original 1st ed. 1981
Springer-Verlag New York Inc.
978-1-4615-9196-2 (ISBN)
CHF 74,85 inkl. MwSt
The first volume in this series is devoted to derivatization techniques in chromatography, for very obvious reasons. In gas chromatography (GC) chemical derivatization as an aid to expand the usefulness of the technique has been known for more than a decade and has become an established approach. The first chapter deals to a great extent with derivatization for the purpose of making compounds amenable to Gc. Although the discussion concentrates on pesticides, some generally valid conclusions can be drawn from this chapter. Chemistry will not be limited to the separation-it can also have a pronounced impact on the sample cleanup, another topic cov­ ered in Chapter 1. Since the introduction of coupled GC-mass spectroscopy (GC-MS), a very powerful tool, derivatization techniques have taken still another di­ rection-taking into consideration chromatographic as well as mass spec­ trometric improvement of the compounds of interest. Cyclic boronates are discussed as derivatization reagents for this purpose in the second chapter.

1. Chemical Derivatization in Pesticide Analysis.- 1. Introduction.- 2. Organochlorine Insecticides.- 3. Organophosphorus Insecticides.- 4. Carbamates (Insecticides and Herbicides).- 5. Herbicides.- 6. Phenols.- 7. Fungicides.- References.- 2. Cyclic Boronates as Derivatives for the Gas Chromatography—Mass Spectrometry of Bifunctional Organic Compounds.- 1. Introduction.- 2. Some Historical Background.- 3. The Scope of Application of Cyclic Boronates in Gas Chromatography.- 4. Gas Chromatographic Properties of Cyclic Boronates.- 5. Mass Spectrometric Properties of Cyclic Boronates.- 6. Preparation of Cyclic Boronates for Use in Gas Chromatography-Mass Spectrometry.- 7. Examples of the Preparation and Gas Chromatography of Cyclic Boronates...- 8. Summary.- References.- 3. General Aspects of Precolumn Derivatization with Emphasis on Pharmaceutical Analysis.- 1. Introduction.- 2. Functional Group Analysis.- 3. Detector Amplification by Paired Ion Chromatography.- 4. Conclusions.- References.- 4. Reaction Detectors in Liquid Chromatography.- 1. Introduction.- 2. Theoretical Aspects.- 3. Technical Aspects and Applications.- 4. Special Applications and Trends.- 5. Conclusions.- References.

Reihe/Serie Modern Analytical Chemistry ; 1
Zusatzinfo XI, 344 p.
Verlagsort New York, NY
Sprache englisch
Maße 155 x 235 mm
Themenwelt Naturwissenschaften Chemie Analytische Chemie
Naturwissenschaften Chemie Physikalische Chemie
ISBN-10 1-4615-9196-1 / 1461591961
ISBN-13 978-1-4615-9196-2 / 9781461591962
Zustand Neuware
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