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Understanding Single-Crystal X-Ray Crystallography - Dennis W. Bennett

Understanding Single-Crystal X-Ray Crystallography

Buch | Softcover
XX, 811 Seiten
2010 | 1. Auflage
Wiley-VCH (Verlag)
978-3-527-32794-2 (ISBN)
CHF 139,95 inkl. MwSt
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Endlich ein Lehrbuch der Röntgenkristallstrukturanalyse von Einkristallen, das ohne weitreichende Vorkenntnisse in Mathematik auskommt! Theorie und methodische Grundlagen werden logisch strukturiert und gut verständlich dargestellt; der Band ist in sich geschlossen und erfordert keine Zusatzliteratur.Für Studenten oberer Semester, Diplomanden und Doktoranden sowie zum Einstieg für Anwender aus allen naturwissenschaftlichen Disziplinen.

Professor Dennis W. Bennett is a Professor of Chemistry and a member of the Laboratory for the Surface Studies at University of Wisconsin in Milwaukee. His research focuses on the physical-inorganic chemistry of molecular devices and catalytic systems. He holds a BS in Biological Sciences and a PhD in Chemistry, both from the University of Utah, where he also did post-doctoral research in photocatalysis. In more recent years, he was a NIH Senior Fellow at the Medical College of Wisconsin, where he gained expertise in macromolecular crystallography. He has also served as Chair of the Department of Chemistry and Biochemistry at UWM, and as a program manager in Basic Energy Services at the U.S. Department of Energy. Prior to his academic career, he was a research chemist at Phillips Petroleum Corp., and has continued to serve as a consultant to a number of companies and government agencies throughout the U.S. He is the author of over 130 peer-reviewed research publications.

CRYSTAL LATTICES
The Solid State
The Crystal Lattice
Vectors in Crystallography
Matrices in Crystallography
Coordinate Systems in Crystallography
CRYSTAL SYMMETRY
Symmetry
Symmetry Group Theory
Point Groups
Space Groups
CRYSTAL DIFFRACTION: THEORY
Electromagnetic Radiation
Diffraction
CRYSTAL DIFFRACTION: EXPERIMENT
The Sphere of Reflection
Recording the Diffraction Pattern: Film Methods
Recording the Diffraction Pattern: Counter Methods
Determining the Orientation Matrix and Unit Cell
Refining the Orientation Matrix and Unit Cell
Determining the Bravais Lattice
The Measurement of Integrated Intensities
CRYSTAL DIFFRACTION: DATA
Experimental Error
Scaling the Intensity Data
Determining the Space Group
CRYSTAL STRUCTURE SOLUTION: EXPERIMENTAL
The Patterson Function
Other Experimental Methods
Completion of the Structural Solution: Fourier Methods
CRYSTAL STRUCTURE SOLUTION: STATISTICAL
Direct Methods
Other Direct Methods
Competion of the Structural Solution: Probability Methods
CRYSTAL STRUCTURE REFINEMENT
Linear Least Squares
Non-Linear Least Squares: Structure Refinement
Macromolecular Refinement
APPENDIX
A Geometric Derivation of Bragg's Law
The Fourier Transform: Electron Density & The Structure Factor
Determination of the Phase Parameter in the Amplitude Reflectivity Ratio
Reflection From a Single Plane
A Discussion of Kinematical Models for Extinction
Probability Integrals: The Modified Bessel Function
Monte Carlo Optimization - A Simple Example
Contrained Optimization
Taylor Series

"This book is the result of many years of research and practical experience, and overall provides not only useful infomration, but also a sense of the author's character that interested readers may also appreciate." ( Materials World , 1 July 2012)
"It is not necessary to follow all the intricate mathematical treatment of matrices, Fourier summation, statistics and so on, in order to derive benefit from the clearly written text and the good range of worked examples". (Chemistry World, 1 January 2011)

Erscheint lt. Verlag 27.1.2010
Sprache englisch
Maße 170 x 240 mm
Gewicht 1560 g
Themenwelt Naturwissenschaften Chemie
Naturwissenschaften Geowissenschaften Mineralogie / Paläontologie
Schlagworte Anorganische Chemie • Biochemie u. Chemische Biologie • Biochemistry (Chemical Biology) • Chemie • Chemistry • crystallography • earth sciences • Geologie u. Geophysik • Geology & Geophysics • Geology & Geophysics • Geowissenschaften • Inorganic Chemistry • Kristallographie • Materials Science • Materialwissenschaften • Physics • Physik • Röntgenkristallographie
ISBN-10 3-527-32794-0 / 3527327940
ISBN-13 978-3-527-32794-2 / 9783527327942
Zustand Neuware
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