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Additional Principles and Methods of Analysis -

Additional Principles and Methods of Analysis (eBook)

Analytical Methods for Pesticides, Plant Growth Regulators, and Food Additives, Vol. 5

Gunter Zweig (Herausgeber)

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2013 | 1. Auflage
590 Seiten
Elsevier Science (Verlag)
978-1-4832-2082-6 (ISBN)
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Analytical Methods for Pesticides, Plant Growth Regulators, and Food Additives, Volume V: Additional Principles and Methods of Analysis covers the major advances in the analytical techniques used for the qualitative and quantitative determinations of minute amounts of pesticide and plant growth regulator residues in foods and crops. The book discusses developments in analytical methods (i.e. the polarographic technique, thin-layer chromatography) and their general applications; the analytical aspects of pesticide residue analyses in the environment; and specific analytical methods for formulation and residue analyses of insecticides, fungicides, herbicides and plant growth regulators. Agriculturists, agricultural engineers, toxicologists, and people involved in the study of pesticides and biochemicals will find the book invaluable.
Analytical Methods for Pesticides, Plant Growth Regulators, and Food Additives, Volume V: Additional Principles and Methods of Analysis covers the major advances in the analytical techniques used for the qualitative and quantitative determinations of minute amounts of pesticide and plant growth regulator residues in foods and crops. The book discusses developments in analytical methods (i.e. the polarographic technique, thin-layer chromatography) and their general applications; the analytical aspects of pesticide residue analyses in the environment; and specific analytical methods for formulation and residue analyses of insecticides, fungicides, herbicides and plant growth regulators. Agriculturists, agricultural engineers, toxicologists, and people involved in the study of pesticides and biochemicals will find the book invaluable.

Front Cover 1
Additional Principles and Methods of Analysis 4
Copyright Page 5
Table of Contents 12
Contributors to Volume V 6
Preface 10
CONTRIBUTORS TO VOLUME V 6
PREFACE 10
PART I: NEWER ANALYTICAL METHODS AND GENERAL APPLICATIONS 22
Chapter 1. Gas Chromatography—Applications and Limitations in Pesticide Residue Analysis 24
I. Introduction 24
II. Limits of Detection 25
III. Chromatographie Columns 27
IV. Detectors 37
V. Guidelines to Pesticide Residue Analysis 58
VI. Notes on Some Problems in Residue Analysis by Gas Chromatography 62
VII. Conclusions 63
References 64
Chapter 2. Thin-Layer Chromatography 68
I. Introduction 68
II. Techniques 72
III. Pesticide Applications 81
IV. Documentation 84
V. Scheme of Analysis 86
References 87
Chapter 3. Polarographic Methods for Pesticides and Additives 88
I. Introduction 88
II. Instrumentation 88
III. Sample Preparation 89
IV. Additives 90
V. Pesticides 93
VI. Conclusion 101
References 101
Chapter 4. Residue Analyses in Water Resources 104
I. Introduction 104
II. Sources of Water-Borne Pesticides 105
III. Pesticide Classification 107
IV. Biological Uptake 109
V. Physical and Chemical Properties 110
VI. Methods of Collection 112
VII. Cleanup of Extract 123
VIII. Pesticide Analysis 127
IX. Analytical Control 132
Acknowledgments 133
References 133
Chapter 5. Principles of Pesticide Metabolism Studies 136
I. Introduction 136
II. Scope 137
III. Methodology 137
IV. Degradation and Metabolism 144
References 164
Chapter 6. Pesticide Analysis in Fish and Wildlife 168
I. Introduction 168
II. Fish and Wildlife Pesticide Problems 168
III. Importance of Pesticide Residue Analyses 170
IV. Exposure of Fish and Wildlife to Pesticides 170
V. Toxicity and Hazard of Pesticides 173
VI. Direct and Indirect Effects of Pesticides 174
VII. Fish and Wildlife Pesticide Studies 176
VIII. Sampling for Pesticide Residue Analysis 183
IX. Analytical Methods 196
X. Presentation of Residue Data 207
References 209
PART II: INSECTICIDES 212
Chapter 7. Azodrin® Insecticide 214
I. General 214
II. Analysis 215
Reference 222
Chapter 8. Banol 224
I. General 224
II. Analysis 225
References 233
Chapter 9. Bidrin® Insecticide 234
I. General 234
II. Analysis 236
References 254
Chapter 10. Binapacryl 256
I. General 256
II. Analysis 257
References 263
Chapter 11. Ciodrin® Insecticide 264
I. General 264
II. Analysis 267
References 277
Chapter 12. Imidan® 278
I. General 278
II. Analysis 279
References 295
Chapter 13. Morestan® 298
I. General 298
II. Analysis 300
References 310
PART III: FUNGICIDES 312
Chapter 14. Difolatan® 314
I. General 314
II. Analysis 316
References 325
Chapter 15. Lanstan® 326
I. General 326
II. Analysis 327
Reference 333
Chapter 16. Pentachlorophenol and Its Sodium Salt 334
I. General 334
II. Analysis 335
References 339
PART IV: ADDITIONAL HERBICIDES AND PLANT GROWTH REGULATORS 340
Chapter 17. Amiben 342
I. General 342
II. Analysis 346
References 355
Chapter 18. Bromacil 356
I. General 356
II. Analyses 357
References 367
Chapter 19. Bromoxynil 368
I. General 368
II. Analysis 374
References 383
Chapter 20. 2,4-Dichlorophenoxyacetic Acid—Newer Methods of Analysis 384
I. General 384
II. Analysis 384
References 388
Chapter 21. 4(2,4-DB) 390
I. General 390
II. Analysis 391
References 394
Chapter 22. Diphenamid 396
I. General 396
II. Analysis 397
References 404
Chapter 23. DNBP 406
I. General 406
II. Analysis 408
References 417
Chapter 24. Diquat 418
I. General 418
II. Analysis 420
References 425
Chapter 25. Duraset® 426
I. General 426
II. Analysis 427
References 432
Chapter 26. Gibberellic Acid 434
I. General 434
II. Analysis 435
References 442
Chapter 27. Ioxynil 444
I. General 444
II. Analysis 449
References 452
Chapter 28. Linuron 454
I. General 454
II. Analyses 455
Reference 458
Chapter 29. MCPA 460
I. General 460
II. Analysis 462
References 475
Chapter 30. Naphthalene Acetic Acid 476
I. General 476
II. Analysis 478
References 487
Chapter 31. Ordram 490
I. General 490
II. Analysis 491
References 493
Chapter 32. Paraquat 494
I. General 494
II. Analysis 496
References 502
Chapter 33. Prefar® 504
I. General 504
II. Analysis 506
References 511
Chapter 34. Ro-Neet® 512
I. General 512
II. Analysis 513
References 518
Chapter 35. Succinic Acid 2,2-Dimethylhydrazide 520
I. General 520
II. Analysis 522
References 526
Chapter 36. Tordon 528
I. General 528
II. Analysis 533
References 545
Chapter 37. Trifluralin 548
I. General 548
II. Analysis 549
References 556
Chapter 38. Vernam® 558
I. General 558
II. Analysis 559
References 562
Author Index 564
Subject Index 573

Erscheint lt. Verlag 22.10.2013
Sprache englisch
Themenwelt Medizin / Pharmazie Gesundheitsfachberufe
Studium 2. Studienabschnitt (Klinik) Pharmakologie / Toxikologie
Naturwissenschaften Biologie
Technik
ISBN-10 1-4832-2082-6 / 1483220826
ISBN-13 978-1-4832-2082-6 / 9781483220826
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