Annual Reports on NMR Spectroscopy (eBook)

Graham A. Webb (Herausgeber)

eBook Download: EPUB

2009 | 1. Auflage
392 Seiten
Elsevier Science (Verlag)
978-0-12-381434-0 (ISBN)

Infos

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy.

* Provides updates on the latest developments in NMR spectroscopy
* Includes comprehensive review articles
* Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

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Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. - Provides updates on the latest developments in NMR spectroscopy- Includes comprehensive review articles- Highlights the increasing importance of NMR spectroscopy as a technique for structural determination

Inhalt

Front cover 1
Annual Reports on NMR Spectroscopy 4
Copyright Page 5
Contents 6
Contributors 8
Preface 10
Chapter 1: Quantitative 2D NMR Studies 12
1. Introduction 13
2. Concepts 15
3. Applications 32
4. Conclusions 37
Acknowledgments 37
References 37
Chapter 2: Recent Advances in Solvent Suppression for Solution NMR: A Practical Reference 44
1. Rationale 45
2. Solvent Suppression 49
3. Suppression Pulse Sequences 63
4. Comparisons, Conclusions, and Advice 78
Acknowledgments 84
Appendix 84
References 85
Chapter 3: Photo-CIDNP Spectroscopy 88
1. Introduction 89
2. CIDNP Phenomena 91
3. CIDNP Theory 93
4. Instrumentation and Techniques 111
5. Chemical Information Obtainable by High-Field CIDNP 121
6. Recent Applications of CIDNP to Chemical and Biochemical Problems 132
7. Conclusions 151
References 151
Chapter 4: Techniques Used for 14N NQR Studies 160
1. Introduction 161
2. Short-repetition Time Sequences in NQR of Nitrogen 162
3. Polarization Enhancement of NQR Signals 179
4. Multi-pulse Sequences Under Conditions of Magneto-acoustic and Piezo-Electric Ringing 183
5. Effect "TNEFMS" in Multi-Pulse 14N NQR 197
6. Conclusion 202
References 203
Chapter 5: Chlorine, Bromine, and Iodine Solid-State NMR Spectroscopy 206
1. Introduction 208
2. Theoretical Background 209
3. Experimental and Computational Methods 218
4. Survey of Available Experimental Data 223
5. Concluding Remarks 326
Acknowledgements 327
References 327
Subject Index 338

Produkt-Details

• Erscheint lt. Verlag: 18.6.2009
• Sprache: englisch
• Themenwelt: Naturwissenschaften ► Chemie ► Analytische Chemie
• Themenwelt: Naturwissenschaften ► Physik / Astronomie ► Elektrodynamik
• Themenwelt: Technik
• ISBN-10: 0-12-381434-0 / 0123814340
• ISBN-13: 978-0-12-381434-0 / 9780123814340